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Instrument Details

Beamline 22‐ID-D

22-ID hutch dewars

Equipment:

  • Detector: Eiger X16M; Dectris
  • Wavelength range: 6.0 - 24.0 keV (approx. 2.1 - 0.52 Angstrom)
  • Minimum crystal-to-detector distance = 150mm
  • Diffractometer: MD3 vertical omega-axis; Arinax
  • Crystal automounter: compatible with MD3
  • 20 Unpick positions with full pin accessibility
  • Additional 10 Unipuck positions with partial pin accessibility (pins 6, 7, 16 out of range)
  • Sample mounting cycle time: TBD
  • Fluorescence detector: Amp-Tek 123 SDD X-ray Spectrometer
  • SERGUI beamline control and data collection software

Beamline 22‐ID-E

22-BM hutch dewar

Equipment:

  • Detector: High-speed MX300-HS; Rayonix
  • Wavelength range: 12.700 keV (approx. 0.97 Angstrom); fixed wavelength
  • Minimum crystal-to-detector = 150mm
  • Diffractometer: MD2 horizontal omega-axis; Arinax
  • Crystal automounter: compatible with MD2
  • 6 Unipuck positions with full pin accessibility
  • Sample mounting cycle time: 30-second dismount/mount cycle
  • Fluorescence detector: Amp-Tek FAST 3DD XR-100 SDD X-ray Detector
  • SERGUI beamline control and data collection software

Beamline Parameters

SER‐CAT

Different optics are available on beamlines 22-ID-D (variable wavelength) and 22-ID-E (fixed wavelength). A table of parameters for both beamlines is given below.

APS graphic crystallography
ParameterBeamline
 22-ID-D22-ID-E
 
 
 
Full Beam Flux (ph/s)
7x10e12
7x10e12
Energy; lower limit (eV)
6,000
 
Energy; upper limit (ev)
24,000
 
Energy; fixed wavelength (eV)
 
12,700
 
 
 
Horizontal beam size; FWHM (microns)
10
10
Vertical beam size; FWHM (microns)
10
10
Aperatures available (microns)
TBD
TBD
 
 
 
Omega range; spindle (degrees)
TBD
TBD
 
 
 
Detector

Dectris

Eiger 16M

Rayonix

MX300HS

Detector distance; minimum (mm)
150mm
150mm
Detector distance; maximum (mm)
TBD
TBD
 
 
 
Number of Uni-pucks; all pin positions accessible
20
6
Number of Uni-pucks; positions 6, 15, 16 inaccessible
10